Rapid Synthesis of Bismuth Molybdate Nanoplates for Supercapacitor Applications by Microwave Combustion Method
A. Shameem1, V. Siva2, A. Murugan3, Shamima Hussain4, S. Asath Bahadur5
1A. Shameem, Department of Physics, Kalasalingam Academy of Research and Education, Krishnankoil (Tamil Nadu), India.
2V. Siva, Department of Physics, Kalasalingam Academy of Research and Education, Krishnankoil (Tamil Nadu), India.
3A. Murugan, Department of Physics, Kalasalingam Academy of Research and Education, Krishnankoil (Tamil Nadu), India.
4Shamima Hussain, UGC-DAE CSR Kalpakkam Node, Kokilamedu, Kalpakkam (Tamil Nadu), India.
5S. Asath Bahadur, Department of Physics, Kalasalingam Academy of Research and Education, Krishnankoil (Tamil Nadu), India.
Manuscript received on 24 November 2019 | Revised Manuscript received on 18 December 2019 | Manuscript Published on 30 December 2019 | PP: 324-328 | Volume-9 Issue-1S4 December 2019 | Retrieval Number: A11741291S419/19©BEIESP | DOI: 10.35940/ijeat.A1174.1291S419
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© The Authors. Blue Eyes Intelligence Engineering and Sciences Publication (BEIESP). This is an open access article under the CC-BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
Abstract: Orthorhombic structured bismuth molybdate (Bi2MoO6 ) is obtained by one pot microwave combustion method. The characteristic performance of Bi2MoO6 nanocatalyst are described by X-ray diffraction (XRD), Scanning Electron Microscopy (SEM) furnished with Energy – dispersive X-ray spectroscopy (EDS) and Fourier change infrared (FT-IR) spectroscopy. The average crystallite size for Bi2MoO6 estimated from XRD is about 28.9 nm. The surface morphology from SEM pictures displays nanoplates. The FTIR is utilized to recognize the structural coordination and the presence of functional group. The electrochemical studies are taken to readily comprehend the electrochemical performance of the modified active electrode with notable specific capacitance value are found 234.9 Fg-1 at 5 mVs-1 and cyclic retention is stable up to 900 cycles (98.7 %). The as-synthesized dynamic material acts as a novel electrode material for supercapacitor.
Keywords: Bi2MoO6, Microwave Combustion Method, Nanoplates, Electrochemical Performance.
Scope of the Article: Microwave Photonics